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A couple of the latest an most well known AJAX frameworks tested and reviewed.
http://www.infoworld.com/article/06/07/31/31FEajax_1.html
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The Web Service Software Factory is a cohesive collection of guidance that enables architects and developers to design and build higher quaility services and achieve more predictable results in less time by applying proven practices and patterns directly within Visual Studio 2005.
http://www.microsoft.com/downloads/details.aspx?familyid=DB996113-6E92-4894-9B7E-0DEBB614D72F&displaylang=en